NAME Solid state NMR platform
Egoera solidoko RMNak material solidoetan molekulen eta ioien egiturari eta dinamikari buruzko informazio oso zehatza eman dezake. Hori askotan funtsezkoa da material berriak ulertzeko eta garatzeko. Egoera solidoko RMNa irismen laburreko ordenarekiko sentikorra den teknika bat da, materialak karakterizatzeko teknika tradizionalak gainditzen dituena, hala nola X izpien difrakzioa edo mikroskopia elektronikoa material amorfoen azterketan, eta teknika horiek osatzen ditu material kristalinoen azterketan. Gainera, RMN solidoak espezifikotasun atomikoa duen informazio dinamikoa eman dezake oso material desordenatuetan, baita guztiz amorfoetan ere. CICen egoera solidoko RMN plataformaren teknologiak material organikoak, inorganikoak eta paramagnetikoak karakterizatzeko diseinatuta daude bereziki, tenperatura aldakorreko azterketak barne (-120 C eta +400 C gradu).
FIELDS OF APPLICATION
Advanced unions
Coatings and Surfaces solutions
Design and development of materials
Manufacturing processes
Materials and processes in Circular Economy
MOST OUTSTANDING EQUIPMENT AND COMPONENTS
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Paramagnetic solid state NMR spectrometer
Low field magnet combined with an ultrafast MAS pobre optimized for the analisis and characterization of paramagnetic solid materials, used for example as cathode in electrochemical devices.
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Solution NMR spectrometer
High resolution 300 MHz BBFO spectrometer equipped with a sample changer for automatized measurements of organic compounds and polymers.
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WB 500 MHz solid state NMR spectrometer
Avance III 500 MHz was installed at CIC in April 2012. It is a wide bore magnet especially suited for non magnetic materials where high resolution is desired. This magnet is equiped with a 1.3mm probe, a triple channel 2.5 mm probe and an static probe for variable temperature studies.
SERVICES OFFERED BY THE ASSET
Analysis of dopants and trace elements
Solid state NMR is suitable for the determination of the presence and the composition of traces of dopants in a material independently of the state of the compound.
Composition
Solid state NMR can determine the composition of a solid material independently of the state of the compound, including amorphous, polymeric, disordered and semi-liquid materials.
Contamination
Solid state NMR can determine the presence of even very small quantities of contaminants in a solid material and help in the understanding of is impact in the material performance.
Corrosion
Solid state NMR can be used to detect and quantify the corrosion of a compound.
Deformulation of unknown compounds and mixtures.
Deformulation of unknown compounds and mixtures.
Material characterization
Solid state NMR can be used to characterize the chemical composition and the physicochemical properties of an unknown material.
Material degradation
Solid state NMR can determine the presence of even very small quantities of side products produced during a material degradation process and help in the understanding of is impact in the material performance.
Variable temperature tests
Our solid state NMR capabilities allow us the measurement of variable temperature experiments. Permitting us the determination of the effects of temperature in the material performance.
ENTITY MANAGING THE ASSET
Contact person:
Leire Olaeta RodrÃguez
lolaeta@cicenergigune.com